A library of C-alkyl and C-aryl nitrones has been obtained by direct condensation of primary Nsubstituted hydroxylamine hydrochlorides with various aldehydes and ketones without catalysts or base. The synthetic procedure, performed under MW irradiation in the absence of solvent, does not require the presence of a base, is fast, clean, high-yielding and characterized by simple work-up.
Rapid, Efficient and Solvent Free Microwave Mediated Synthesis of Aldo- and Ketonitrones
NARDI M;
2016-01-01
Abstract
A library of C-alkyl and C-aryl nitrones has been obtained by direct condensation of primary Nsubstituted hydroxylamine hydrochlorides with various aldehydes and ketones without catalysts or base. The synthetic procedure, performed under MW irradiation in the absence of solvent, does not require the presence of a base, is fast, clean, high-yielding and characterized by simple work-up.File in questo prodotto:
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