A fast and versatile microwave-(MW)-assisted method for the post-calcination functionalization of MCM-41 is proposed. The efficiency of the grafting is improved in the absence of solvent and depends on the MW-heating time. Moreover, working under the same reaction conditions, the organic loadings strictly depend on the silylating agent.
General MW-assisted grafting of MCM-41: Study of the dependence on time dielectric heating and solvent
NARDI M;
2009-01-01
Abstract
A fast and versatile microwave-(MW)-assisted method for the post-calcination functionalization of MCM-41 is proposed. The efficiency of the grafting is improved in the absence of solvent and depends on the MW-heating time. Moreover, working under the same reaction conditions, the organic loadings strictly depend on the silylating agent.File in questo prodotto:
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